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- W2045001517 abstract "Monodisperse silica particles (SiPs) of diameter between 100 and 1500 nm were surface-modified in a mixture of ethanol/water/ammonia with a newly designed triethoxysilane having an atom transfer radical polymerization (ATRP) initiating site, (2-bromo-2-methyl)propionyloxyhexyltriethoxysilane. The surface-initiated ATRP of methyl methacrylate (MMA) mediated by a copper complex was carried out with the initiator-fixed SiPs in the presence of a “sacrificial” (free) initiator. The polymerization proceeded in a living manner in all examined cases, producing SiPs coated with well-defined PMMA of a target molecular weight up to 480K with a graft density as high as 0.65 chains/nm2. These hybrid particles had an exceptionally good dispersibility in organic solvents. Transmission electron microscopic and atomic force microscopic observations of their monolayers prepared at the air−water interface revealed that they formed an ordered 2-dimensional lattice extending throughout the monolayer." @default.
- W2045001517 created "2016-06-24" @default.
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- W2045001517 date "2005-02-09" @default.
- W2045001517 modified "2023-10-10" @default.
- W2045001517 title "Synthesis of Monodisperse Silica Particles Coated with Well-Defined, High-Density Polymer Brushes by Surface-Initiated Atom Transfer Radical Polymerization" @default.
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- W2045001517 doi "https://doi.org/10.1021/ma048011q" @default.
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