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- W2045181206 abstract "Simple procedures to synthesize a variety of 14C-labeled monomeric and polymeric siloxanes are described. Specifically, the synthesis of the following siloxanes, some of which are of significant commercial importance are provided: 14C-octamethylcyclotetrasiloxane (D4), 14C-decamethylcyclopentasiloxane (D5), 14C-hexamethyldisiloxane (MM), 14C-dimethyldimethoxysilane and 14C-dimethylsilanediol (DMSD) are examples of discrete monomeric species. 14C-350 and 1000 cSt polydimethylsiloxanes (PDMS) are examples of polymeric species. Synthesis of the monomeric species with the exception of dimethylsilanediol involve reactions of Grignard reagents with the appropriate chlorosilanes, while the polymeric materials were synthesized via acid catalyzed equilibration reaction of 14C-D4 with dodecamethylpentasiloxane (MD3M). The compound 14C-DMSD was obtained by the hydrolysis of 14C-dimethyldimethoxysilane. The labeled materials listed here were synthesized for their utility as tracers in several of the ongoing environmental fate and effects studies as well as toxicological investigations." @default.
- W2045181206 created "2016-06-24" @default.
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- W2045181206 date "1999-01-01" @default.
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- W2045181206 title "Synthesis of 14C-labeled cyclic and linear siloxanes" @default.
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- W2045181206 doi "https://doi.org/10.1016/s0022-328x(98)00916-4" @default.
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