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- W2045186315 abstract "The reaction of 2-amino-4,5-dimethyl- thiophene-3-carboxamide with iso(and isothio) cyanates for the synthesis of thieno[2,3-d]pyrimidines has been investigated. The reactions under microwave irradiation in the presence of N,N-dimethyl acetamide as solvent gave 5,6-dimethylthieno[2,3-d]pyrimidine-2,4(1H,3H)-dione, 5,6-dimethyl-2-thioxo-2,3-dihy- drothieno[2,3-d]pyrimidin-4(1H)-one, and 2-aryla- mino-5,6-dimethylthieno[2,3-d]pyrimidin-4(3H)-one derivatives. These reactions probably proceed through intermediates 4,5-dimethyl-2-substitutedcarbamoth- ioylaminothiophene-3-carboxamides. Two of these intermediates were isolated. © 2009 Wiley Periodicals, Inc. Heteroatom Chem 20:346–349, 2009; Published online in Wiley InterScience (www.interscience.wiley.com). DOI 10.1002/hc.20557" @default.
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- W2045186315 date "2009-01-01" @default.
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- W2045186315 title "Investigation into the reaction of 2-amino-4,5-dimethylthiophene-3-carboxamide with iso(and isothio)cyanates under microwave irradiation" @default.
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