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- W2045242854 abstract "Determination of the degree of substitution, D.S., of purified sodium carboxymethylcellulose, CMC, by potentiometric titration has been studied. Different mathematical descriptions of the acid-base properties of polyelectrolytes were tested on the titration curve. It was found that the extended Henderson-Hasselbalch equation reproduced the measured data well. It was therefore used as a basis for evaluating D.S. by the simplex method. The influence of ionic strength, I, on the shape of the titration curve was investigated and the effect of I on the precision of the titrations was evaluated. The titrations showed a precision of ± 0.004 D.S.-units and the results were in agreement with those obtained from a dry-ashing method, within ± 0.02 D.S.-units. The whole method, including preparation of solutions and titration, showed a precision of ± 0.01 D.S.-units." @default.
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- W2045242854 date "1985-08-01" @default.
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- W2045242854 title "Determination of the degree of substitution of sodium carboxymethylcellulose by potentiometric titration and use of the extended henderson-hasselbalch equation and the simplex method for the evaluation" @default.
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- W2045242854 doi "https://doi.org/10.1016/0039-9140(85)80160-0" @default.
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