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- W2045268148 abstract "Abstract By using a precursor complex [Fe 3 O(PhCO 2 ) 6 (H 2 O) 3 ]NO 3 as starting material and 2,2′‐bpy (= 2,2′‐bipyridine) as rigid chelating ligand, the new dinuclear iron‐oxido complex [Fe 2 O(PhCO 2 ) 2 (2,2′‐bpy) 2 (N 3 ) 2 ] · H 2 O ( 1 ) was synthesized and structurally characterized. The reaction of [Fe 3 O(PhCO 2 ) 6 (H 2 O) 3 ]NO 3 with 2,2′‐bpy and sodium azide in 1:3:3 ratio gave the dinuclear complex 1 , whereas a 1:6:3 ratio reaction system only gave the complex [Fe(2,2′‐bpy) 3 ] 3+ , which indicated that 2,2′‐bipyridine plays a crucial function in the nuclear forming procedure. Meanwhile, the N 3 – ligands take up the chelating domain of oxygen and reduce the nucleation. Different π–π interactions exist in 1 , which extend its structure to a three dimensional supramolecular framework." @default.
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- W2045268148 date "2010-11-01" @default.
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- W2045268148 title "Synthesis and Crystal Structure of a New Dinuclear Iron(III) Complex: [Fe<sub>2</sub>O(PhCO<sub>2</sub>)<sub>2</sub>(2,2′‐bpy)<sub>2</sub>(N<sub>3</sub>)<sub>2</sub>]·H<sub>2</sub>O" @default.
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