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- W2045378410 abstract "Monodisperse oligo[(1,4-phenyleneethynylene)-alt-(2,5-thiopheneethynylene)]s were synthesized via an iterative divergent/convergent doubling strategy on resin. Thus, the resin-supported terminal acetylene 1 reacted with compound 2 in the presence of Pd/Cu catalyst to give the desired ‘starting monomer’ 3 for the iterative divergent/convergent doubling strategy. One third of 3 was subjected to desilylation with TBAF to give the resin 4. Two thirds of 3 were treated with MeI to afford 5 in 77% yield. Resin 4 reacted with 5 in the presence of Pd/CuI to give resin 6. The sequence was repeated to generate resin 9, which was treated with MeI to give octamer 10 in 37% yield over three steps." @default.
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- W2045378410 date "2006-06-01" @default.
- W2045378410 modified "2023-10-17" @default.
- W2045378410 title "Solid-Phase Synthesis of Oligo[(1,4-phenyleneethynylene)-alt-(2,5-thiopheneethynylene)]s" @default.
- W2045378410 doi "https://doi.org/10.1055/s-2006-941795" @default.
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