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• W2045388081 endingPage "2431" @default.
• W2045388081 startingPage "2423" @default.
• W2045388081 abstract "The reaction of in situ generated 1′-(diphenylphosphino)-1-lithioferrocene with isocyanates RNCO affords the respective phosphino-carboxamides Ph2PfcCONHR (fc = ferrocene-1,1′-diyl, R = cyclohexyl (2), and Ph (3)) in moderate yields. The coordination behaviour of 3 chosen as a representative was studied in palladium(II) and platinum(II) complexes. Depending on the metal precursor and the reaction conditions, the following compounds featuring this ligand as a P-monodentate or an O,P-chelating donor were isolated and characterised by spectroscopic methods (IR, multinuclear NMR and electrospray ionisation MS): trans-[PdCl2(3-κP)2] (5), trans-[PtCl2(3-κP)2] (6), cis-[PtCl2(3-κP)2] (7), [SP-4-4]-[(LNC)PdCl(3-κP)] (8; LNC = 2-[(dimethylamino-κN)methyl]phenyl-κC1), and [SP-4-3]-[(LNC)PdCl(3-κ2O,P)]SbF6 (9). Besides, the crystal structures of a phosphine oxide resulting by oxidation of 2, viz Ph2P(O)fcCONHCy (4), and of complexes 5·2Et2O and 9 have been determined by single-crystal X-ray diffraction analysis." @default.
• W2045388081 created "2016-06-24" @default.
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• W2045388081 creator A5059980683 @default.
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• W2045388081 date "2010-10-01" @default.
• W2045388081 modified "2023-10-11" @default.
• W2045388081 title "Preparation of phosphinoferrocene carboxamides from isocyanates. Synthesis and structural characterisation of palladium(II) and platinum(II) complexes with 1′-(diphenylphosphino)-1-(N-phenylcarbamoyl)ferrocene" @default.
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• W2045388081 doi "https://doi.org/10.1016/j.jorganchem.2010.07.013" @default.
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