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- W2045433044 abstract "5-O-α-d-Glucopyranosyl-β-d-fructopyranose (leucrose,1) was transformed into 3,4-di-O-acetyl-1-O-methanesulfonyl-5-O-(2,3,4-tri-O-acetyl-6-O-methanesulfonyl-α-d-glucopyranosyl)-β-d- fructopyranosyl bromide (3) and 1,3,4-tri-O-benzoyl-5-O-(2,3,4,6-tetra-O-benzoyl-α-d-glucopyranosyl)-β-d-fructopyranosyl bromide (8), which were converted into derivatives (8 and9) of 2,6-anhydro-1-deoxy-5-O-α-d-glucopyranosyl-d-arabino-hex-1-enitol. Hydrogenation of8 and9 gave the corresponding anhydroalditol derivatives.N-Iodosuccinimide-mediated glycosylation of9 with 1,2,3,4-tetra-O-acetyl-β-d-glucopyranose gave 1,2,3,4-tetra-O-acetyl-6-O-[3,4-di-O-benzoyl-1-deoxy-1-iodo-5-O-(2,3,4,6-tetra-O-benzoyl-α-d-glucopyranosyl)-β-d- fructopyranosyl]-β-d-glucopyranose (12). Some amino, acetylated, and isopropylidene derivatives of leucrose have been prepared and characterised." @default.
- W2045433044 created "2016-06-24" @default.
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- W2045433044 date "1990-09-01" @default.
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- W2045433044 title "Synthesis and reactions of leucrose and its exocyclic glycal" @default.
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- W2045433044 doi "https://doi.org/10.1016/0008-6215(90)80151-r" @default.
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