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• W2045703100 abstract "Manganese meso-tetra (4-nitrophenyl)porphyrin (Mn-TNPP) with four nitro groups at periphery was employed as building moieties to condense with p-phenylenediamine and benzidine into extended π materials, respectively. Two covalent metalloporphyinic polymers (CMPs) linked by azo (NN) were denoted as azo-CMP-1 and azo-CMP-2. FT-IR, XRD, SEM, TG, contact angle (CA) and XPS were used to analyze and characterize the synthesized heterogeneous materials. The catalytic study has demonstrated that azo-CMP catalysts displayed an excellent performance for epoxidation of olefins, especially cyclohexene. When azo-CMP-1 was recycled five times, its catalytic activity remained with an inconspicuous decrease. Additionally, azo-CMP series exhibited a amphipathic property evidenced by CA test, facilitating the diffusion of reactant into channels of azo-CMPs. Furthermore, the peak value of Mn2p3/2 shifting to a higher value for azo-CMP-1 suggested that there was a catalysis-promoted electronic environment around the Mn(III) active sites, compared to either azo-CMP-2 or homogenous sites." @default.
• W2045703100 created "2016-06-24" @default.
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• W2045703100 date "2015-01-01" @default.
• W2045703100 modified "2023-10-16" @default.
• W2045703100 title "Directing two azo-bridged covalent metalloporphyrinic polymers as highly efficient catalysts for selective oxidation" @default.
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• W2045703100 doi "https://doi.org/10.1016/j.apcata.2014.10.023" @default.
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