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• W2045758217 abstract "Abstract The hydrido complexes [ReH(Cl)(N–N)P 3 ]BPh 4 [P = PPh(OEt) 2 ; N–N = 2,2′‐bipyridine (bpy), 5,5′‐dimethylbipyridine (5,5′‐Me 2 bpy), 1,10‐phenanthroline (phen)] have been prepared by allowing ReCl 3 P 3 to react with the polypyridine in refluxing ethanol. The dihydrido [ReH 2 (bpy)P 3 ]BPh 4 complex has also been prepared by treating [ReHCl(bpy)P 3 ] + cation with NaBH 4 in ethanol. Similarly, the hydrido tricarbonyl derivative [ReH 2 (bpy)(CO) 3 ]BPh 4 has been synthesized by allowing [ReH(bpy)(CO) 3 ] to react with HBF 4 · Et 2 O. All complexes have been characterized spectroscopically (IR and NMR spectroscopic data) and the [ReHCl(bpy){PPh(OEt) 2 } 3 ]BPh 4 derivative by X‐ray crystallography. Protonation of both [ReHCl(bpy)P 3 ]BPh 4 and [ReH 2 (bpy)P 3 ]BPh 4 with HBF 4 · Et 2 O leads to the classical cations [ReH 2 Cl(bpy)P 3 ] 2+ and [ReH 3 (bpy)P 3 ] 2+ , respectively. The vinyl complexes [Re{CH=C(H)R} 2 (bpy)P 3 ]BPh 4 (R = Ph, p ‐tolyl, tert ‐butyl) have also been prepared by allowing the dihydrido derivative [ReH 2 (bpy)P 3 ]BPh 4 to react with an excess of terminal alkyne in 1,2‐dichloroethane.(© Wiley‐VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, Germany, 2007)" @default.
• W2045758217 created "2016-06-24" @default.
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• W2045758217 date "2007-04-01" @default.
• W2045758217 modified "2023-10-18" @default.
• W2045758217 title "Preparation and Reactivity of Hydridorhenium Complexes with Polypyridine and Phosphonite Ligands" @default.
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• W2045758217 doi "https://doi.org/10.1002/ejic.200601056" @default.
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