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- W2045792064 abstract "We describe a practical synthesis of protected (3S,6R)-6-hydroxy-cyclolysine derivatives starting from cyclic l-lysine. Evaluation of the electrochemical oxidation of various protected amino-caprolactams allowed a regioselective electromethoxylation at the α-position to the lactam nitrogen. Formation of the corresponding enamide by elimination of methanol followed by a diastereoselective dihydroxylation, diacetylation and subsequent regioselective reduction afford the orthogonally protected (3S,6R)-3-amino-6-hydroxy-azepan-2-one." @default.
- W2045792064 created "2016-06-24" @default.
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- W2045792064 date "2004-01-01" @default.
- W2045792064 modified "2023-10-18" @default.
- W2045792064 title "Electrooxidation Based Strategy Towards the Core 3-Amino-6-Hydroxyazepan-2-one" @default.
- W2045792064 doi "https://doi.org/10.1055/s-2004-820048" @default.
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