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• W2045850622 abstract "We successfully completed the total synthesis of kulokekahilide-2, a cytotoxic depsipeptide from the Cephalaspiedean mollusk Phillinopsis speciosa. We have revised the absolute stereochemistry of kulokekahilide-2 to 21-l-Ala, 24-d-MePhe, 37-l-Ile, 43-d-Ala, 15-d-Hica, and 5S,6S,7S-Dtda. We also investigated the cause of the mis-assignment of the configuration in the originally proposed kulokekahilide-2 and concluded that methanolysis using MeONa caused partial racemization, which led to the mis-assignment. The structure–activity relationships of kulokekahilide-2 and its analogs indicate the importance of an l-amino acid at position 21." @default.
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• W2045850622 date "2012-01-01" @default.
• W2045850622 modified "2023-10-18" @default.
• W2045850622 title "The total synthesis and structure–activity relationships of a highly cytotoxic depsipeptide kulokekahilide-2 and its analogs" @default.
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• W2045850622 doi "https://doi.org/10.1016/j.tet.2011.10.094" @default.
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