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- W2045888911 abstract "Abstract Treatment of 3′-fluoro-3′-deoxythymidine (FLT), 3′-azido-3′-deoxythymidine (AZT) and 2′,3′-dideoxyadenosine (ddA) with tris(1,1,1,3,3,3-hexafluoro-2-propyl)phosphite or phosphorous acid and N,N'-dicyclohexylcarbodiimide produced the corresponding nucleoside 5′-hydrogenphosphonates. Reaction of FLT, AZT and 3′-deoxythymidine (ddT) with fluorophosphoric acid and 2,4,6-triisopropylbenzenesulfonyl chloride lead to the corresponding nucleoside 5′-phosphorofluoridates also on a multi-gram scale. All the compounds were isolated in high pure state by chromatographic technique." @default.
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- W2045888911 date "1993-12-01" @default.
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- W2045888911 title "A Simple Multi-Gram Synthesis of 5′-Hydrogenphosphonates and 5′-Phosphorofluoridates of Sugar Modified Nucleosides" @default.
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