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• W2046005414 abstract "We have investigated analysis of anion radicals of phenanthrenequinone (PhQ) and anthraquinone (AQ) using acetonitrile-capillary electrophoresis (CE) under anaerobic conditions. PhQ and AQ have relatively high negative reduction potentials meaning that their anion radicals are re-oxidized quite readily by the surrounding O(2) to disappear during analysis and we failed to detect them with our previous system. In this work, we have developed an on-line system combining a unique electrolysis cell for generation of the radicals and a CE unit to keep the analysis system free from external O(2) molecules and to reduce analysis time remarkably. As a result, electrophoretic detection of the anion radicals of PhQ and AQ has been achieved. Furthermore, we have observed hydrogen-bonding interaction between the anion radicals and dimethylurea (DMU) using the present system and have indicated a characteristic interaction of the anion radical of PhQ as an ortho-quinone with DMU." @default.
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• W2046005414 date "2003-05-01" @default.
• W2046005414 modified "2023-09-27" @default.
• W2046005414 title "Electrophoretic analysis of quinone anion radicals in acetonitrile solutions using an on-line radical generator" @default.
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• W2046005414 doi "https://doi.org/10.1002/elps.200305395" @default.
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