FRINK Linked Data Fragments server

Matches in SemOpenAlex for { <https://semopenalex.org/work/W2046147773> ?p ?o ?g. }

• W2046147773 endingPage "566" @default.
• W2046147773 startingPage "558" @default.
• W2046147773 abstract "A simple and specific method able to identify and quantify traces of 14 sulfonamide antibacterials (SAs) in milk and eggs is presented. This method uses a single solid-phase extraction (SPE) cartridge for simultaneous extraction and purification of SAs in the above matrices. Milk and egg samples are passed through a Carbograph 4 sorption cartridge. After analyte desorption, an aliquot of the final extract is injected into a liquid chromatography−mass spectrometry (LC-MS) instrument equipped with an electrospray ion source (ESI) and a single quadrupole. MS data acquisition is performed in the positive-ion mode and by a time-scheduled multiple-ion selected ion monitoring program. Compared to two published methods, the present protocol extracted larger amounts of SAs from both milk and egg and decreased the analysis time by a factor of 3 with milk samples and by a factor of 2 with egg samples. Recovery of SAs in milk at the 5 ppb level ranged between 76 and 112% with relative standard deviations (RSDs) of ⩽13%. Recovery of SAs in egg at the 50 ppb level ranged between 68 and 106% with RSDs of ≤12%. Estimated limits of quantification (S/N = 10) of the method were 1−6 ppb of SAs in whole milk and 5−13 ppb of SAs in eggs. Analyses of eggs from three layer chickens treated with sulfoquinoxaline revealed this antibacterial was still present at the 150 ppb level 1 week after withdrawal. Keywords: Sulfonamides; milk; egg; SPE extraction; LC-MS" @default.
• W2046147773 created "2016-06-24" @default.
• W2046147773 creator A5017269214 @default.
• W2046147773 creator A5023435774 @default.
• W2046147773 creator A5027072069 @default.
• W2046147773 creator A5052564556 @default.
• W2046147773 creator A5080121346 @default.
• W2046147773 date "2002-12-18" @default.
• W2046147773 modified "2023-09-26" @default.
• W2046147773 title "A Simple and Sensitive Liquid Chromatography−Mass Spectrometry Confirmatory Method for Analyzing Sulfonamide Antibacterials in Milk and Egg" @default.
• W2046147773 cites W1519011873 @default.
• W2046147773 cites W1970739657 @default.
• W2046147773 cites W1980595924 @default.
• W2046147773 cites W1987973138 @default.
• W2046147773 cites W1998674651 @default.
• W2046147773 cites W2007784354 @default.
• W2046147773 cites W2009644786 @default.
• W2046147773 cites W2012820552 @default.
• W2046147773 cites W2022137154 @default.
• W2046147773 cites W2033953444 @default.
• W2046147773 cites W2061939981 @default.
• W2046147773 cites W2101390691 @default.
• W2046147773 cites W2121545158 @default.
• W2046147773 cites W2171710890 @default.
• W2046147773 cites W4300755522 @default.
• W2046147773 doi "https://doi.org/10.1021/jf020834w" @default.
• W2046147773 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/12537423" @default.
• W2046147773 hasPublicationYear "2002" @default.
• W2046147773 type Work @default.
• W2046147773 sameAs 2046147773 @default.
• W2046147773 citedByCount "52" @default.
• W2046147773 countsByYear W20461477732012 @default.
• W2046147773 countsByYear W20461477732013 @default.
• W2046147773 countsByYear W20461477732015 @default.
• W2046147773 countsByYear W20461477732017 @default.
• W2046147773 countsByYear W20461477732018 @default.
• W2046147773 countsByYear W20461477732019 @default.
• W2046147773 crossrefType "journal-article" @default.
• W2046147773 hasAuthorship W2046147773A5017269214 @default.
• W2046147773 hasAuthorship W2046147773A5023435774 @default.
• W2046147773 hasAuthorship W2046147773A5027072069 @default.
• W2046147773 hasAuthorship W2046147773A5052564556 @default.
• W2046147773 hasAuthorship W2046147773A5080121346 @default.
• W2046147773 hasConcept C10390740 @default.
• W2046147773 hasConcept C106848363 @default.
• W2046147773 hasConcept C161176658 @default.
• W2046147773 hasConcept C162356407 @default.
• W2046147773 hasConcept C179302884 @default.
• W2046147773 hasConcept C185592680 @default.
• W2046147773 hasConcept C191897082 @default.
• W2046147773 hasConcept C192562407 @default.
• W2046147773 hasConcept C194451485 @default.
• W2046147773 hasConcept C205345274 @default.
• W2046147773 hasConcept C2775926907 @default.
• W2046147773 hasConcept C2778576202 @default.
• W2046147773 hasConcept C34381374 @default.
• W2046147773 hasConcept C43617362 @default.
• W2046147773 hasConcept C4725764 @default.
• W2046147773 hasConcept C6557445 @default.
• W2046147773 hasConcept C81426234 @default.
• W2046147773 hasConcept C86803240 @default.
• W2046147773 hasConceptScore W2046147773C10390740 @default.
• W2046147773 hasConceptScore W2046147773C106848363 @default.
• W2046147773 hasConceptScore W2046147773C161176658 @default.
• W2046147773 hasConceptScore W2046147773C162356407 @default.
• W2046147773 hasConceptScore W2046147773C179302884 @default.
• W2046147773 hasConceptScore W2046147773C185592680 @default.
• W2046147773 hasConceptScore W2046147773C191897082 @default.
• W2046147773 hasConceptScore W2046147773C192562407 @default.
• W2046147773 hasConceptScore W2046147773C194451485 @default.
• W2046147773 hasConceptScore W2046147773C205345274 @default.
• W2046147773 hasConceptScore W2046147773C2775926907 @default.
• W2046147773 hasConceptScore W2046147773C2778576202 @default.
• W2046147773 hasConceptScore W2046147773C34381374 @default.
• W2046147773 hasConceptScore W2046147773C43617362 @default.
• W2046147773 hasConceptScore W2046147773C4725764 @default.
• W2046147773 hasConceptScore W2046147773C6557445 @default.
• W2046147773 hasConceptScore W2046147773C81426234 @default.
• W2046147773 hasConceptScore W2046147773C86803240 @default.
• W2046147773 hasIssue "3" @default.
• W2046147773 hasLocation W20461477731 @default.
• W2046147773 hasLocation W20461477732 @default.
• W2046147773 hasOpenAccess W2046147773 @default.
• W2046147773 hasPrimaryLocation W20461477731 @default.
• W2046147773 hasRelatedWork W1964649783 @default.
• W2046147773 hasRelatedWork W1990426173 @default.
• W2046147773 hasRelatedWork W1997239483 @default.
• W2046147773 hasRelatedWork W2002567025 @default.
• W2046147773 hasRelatedWork W2007802584 @default.
• W2046147773 hasRelatedWork W2011881576 @default.
• W2046147773 hasRelatedWork W2057706260 @default.
• W2046147773 hasRelatedWork W2144071467 @default.
• W2046147773 hasRelatedWork W2761385196 @default.
• W2046147773 hasRelatedWork W2519058244 @default.
• W2046147773 hasVolume "51" @default.
• W2046147773 isParatext "false" @default.
• W2046147773 isRetracted "false" @default.
• W2046147773 magId "2046147773" @default.

• next