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- W2046152893 abstract "Starting from (-)-camphor-10-sulfonic acid (5) the crystalline sultam 9 was readily prepared. TiCl4-mediated Diels-Alder addition of the N-crotonoyl sultam 11 to cyclopentadiene, crys- tallization of the resulting adduct 12 and subsequent reduction gave virtually pure (1S, 4R, 5R, 6S)-1 together with recovered auxiliary 9. The loganin precursor 1 was transformed into norbornanone 20, which upon Baeyer-Villiger oxidation led to the suitably substituted cyclo- pentane 22 from which 1-B-O-methyl loganin aglucone (2) was rea- dily available." @default.
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- W2046152893 date "1986-01-01" @default.
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- W2046152893 title "Iridoids : enantioselective synthesis of loganin via an asymmetric diels-alder reaction" @default.
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- W2046152893 doi "https://doi.org/10.1016/s0040-4020(01)87559-1" @default.
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