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• W2046167576 abstract "A new diimide–diacid chloride (3) containing a noncoplanar 2,2′-dimethyl-4,4′-biphenylene unit was synthesized by treating 2,2′-dimethyl-4,4′-diamino-biphenylene with trimellitic anhydride followed by refluxing with thionyl chloride. Various new poly(ester-imide)s were prepared from 3 with different bisphenols by solution polycondensation in nitrobenzene using pyridine as hydrogen chloride quencher at 170°C. Inherent viscosities of the poly(ester-imide)s were found to range between 0.31 and 0.35 dL g−1. All of the poly(ester-imide)s, except the one containing pendent adamantyl group 5e, exhibited excellent solubility in the following solvents: N,N-dimethylformamide, tetrahydrofuran, tetrachloroethane, dimethyl sulfoxide, N,N-dimethylacetamide, N-methyl-2-pyrrolidinone, m-cresol, o-chlorophenol, and chloroform. The polymers showed glass-transition temperatures between 166 and 226°C. The 10% weight loss temperatures of the poly(ester-imide)s, measured by TGA, were found to be in the range between 415 and 456°C in nitrogen. © 2004 Wiley Periodicals, Inc. J Appl Polym Sci 92: 2486–2493, 2004" @default.
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• W2046167576 date "2004-01-01" @default.
• W2046167576 modified "2023-10-05" @default.
• W2046167576 title "Synthesis and characterization of new soluble poly(ester-imide)s containing noncoplanar 2,2?-dimethyl-4,4?-biphenylene unit" @default.
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• W2046167576 doi "https://doi.org/10.1002/app.20173" @default.
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