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• W2046193064 abstract "Homobrexan-2-one was synthesized labeled in the α-position with 13C and also with an axial or equatorial D. Their p-tosylhydrazone Li salts were thermolyzed and photolyzed (Bamford-Stevens reaction) to generate putative singlet carbenes, which undergo competitive 1,3-insertion to a @Tetracycle and 1,2-H (or D) shift to an alkene. After correction for isotope effects, the Hax/Heq shift ratios were ca. 1.7 and ca. 1.2 for the thermal and photic processes, respectively. These ratios are free of chair-boat and epimerization ambiguities." @default.
• W2046193064 created "2016-06-24" @default.
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• W2046193064 creator A5051650488 @default.
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• W2046193064 date "1993-09-01" @default.
• W2046193064 modified "2023-10-16" @default.
• W2046193064 title "Hydrogen migrations in a constrained cyclohexylidene. Hax/Heq shift ratios in thermal and photic Bamford-Stevens reactions." @default.
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• W2046193064 doi "https://doi.org/10.1016/s0040-4020(01)88030-3" @default.
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