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- W2046206419 abstract "Abstract 3‐Hydroxy‐5‐methylphthalates are prepared by regioselective chelation‐controlled cyclization of 1,3‐bis(silyloxy)‐1,3‐butadienes with 4‐silyloxy‐2‐oxo‐3‐butenoates derived from acetylpyruvates. The employment of silylated benzoylpyruvates instead of acetylpyruvates results in a regioselectivity change and the formation of 6‐aryl‐2‐hydroxyterephthalates. The cyclization of 1,3‐bis(silyloxy)‐1,3‐butadienes with 4‐ethoxy‐2‐oxo‐3‐butenoates, readily available by condensation of enol ethers with methyl 2‐chloro‐2‐oxoacetate, provides a convenient approach to 2‐hydroxyterephthalates and 3‐hydroxyphthalates depending on the substitution pattern of the diene." @default.
- W2046206419 created "2016-06-24" @default.
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- W2046206419 date "2010-06-22" @default.
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- W2046206419 title "Competing Regiodirecting Effects of Ester and Aryl Groups in [3+3] Cyclocondensations of 1,3-Bis(trimethylsilyloxy)-1,3-butadienes: Regioselective Synthesis of 3-Hydroxyphthalates and 2-Hydroxyterephthalates" @default.
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- W2046206419 doi "https://doi.org/10.1002/ejoc.200901373" @default.
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