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• W2046234328 abstract "The Driven Equilibrium Fourier Transform (DEFT) technique for signal enhancement in pulsed 13C magnetic resonance spectroscopy has been investigated for several small 60%-enriched molecules. The experimental results demonstrate that enhancements in signal/noise over the conventional repetitive single-pulse method are indeed obtainable but are much lower than originally predicted. The principal reason is the fact that T2 < T1 for 13C nuclei in most compounds due to transverse relaxation contributions from 13CH scalar coupling, and the experimental data presented here agree well with calculations for the case where T2 < T1. In practice, magnetic field instabilities may limit the enhancements attainable with pulse spacings large enough to allow sufficient resolution in the final Fourier-transformed spectrum." @default.
• W2046234328 created "2016-06-24" @default.
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• W2046234328 date "1972-12-01" @default.
• W2046234328 modified "2023-10-04" @default.
• W2046234328 title "The driven equilibrium fourier transform NMR technique: An experimental study" @default.
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• W2046234328 doi "https://doi.org/10.1016/0022-2364(72)90046-7" @default.
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