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- W2046245655 abstract "Abstract We identified three metal(II) salts of cyameluric acid, namely CaNH 4 (H 2 C 6 N 7 O 3 )(HC 6 N 7 O 3 )·6H 2 O, [Cu(NH 3 ) 2 ] 3 (C 6 N 7 O 3 ) 2 ·2H 2 O and (NH 4 ) 2 [Zn(H 2 O) 6 ](HC 6 N 7 O 3 ) 2 ·2H 2 O. All three compounds were prepared by crystallization from aqueous ammonia solutions containing the respective metal(II) ions. Apparently, the copper salt is identical with a compound claimed in the literature with formula CuNH 4 C 6 N 7 O 3 ·NH 3 . We studied the structure of all three compounds using single‐crystal XRD ( CaNH 4 (H 2 C 6 N 7 O 3 )(HC 6 N 7 O 3 )·6H 2 O : P bar{1} (no. 2), a = 6.6428(13), b = 8.7159(17), c = 19.245(4) Å, α = 92.52(3), β = 92.22(3), γ = 106.95(3)°, V = 1063.3(4) Å 3 , Z = 2), ( [Cu(NH 3 ) 2 ] 3 (C 6 N 7 O 3 ) 2 ·2H 2 O : P bar{1} (no. 2), a = 7.1732(14), b = 9.2338(18), c = 9.994(2) Å, α = 94.15(3), β = 106.13(3), γ = 106.28(3)°, V = 602.3(3) Å 3 , Z = 1), ( (NH 4 ) 2 [Zn(H 2 O) 6 ](HC 6 N 7 O 3 ) 2 ·2H 2 O : P bar{1} (no. 2), a = 6.7568(14), b = 8.7252(17), c = 10.505(2) Å, α = 77.03(3), β = 77.08(3), γ = 82.95(3)°, V = 586.5(2) Å 3 , Z = 1). With the present work we provide the first structural investigation of cyamelurate salts containing divalent metal ions. We studied the occurrence of special structural features for the title compounds which have been claimed for copper salts of cyameluric acid by earlier works. We also made some fundamental discoveries about the crystal growth in these systems. The copper compound was studied further, using magnetic measurements and thermal analysis." @default.
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- W2046245655 date "2009-10-01" @default.
- W2046245655 modified "2023-10-10" @default.
- W2046245655 title "Metal(II) Cyamelurates Prepared from Aqueous Ammonia" @default.
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- W2046245655 doi "https://doi.org/10.1002/zaac.200900130" @default.
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