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• W2046255364 abstract "A new two-dimensional-layered fluoroaluminophosphate (C4H11NOH)3.5[Al4(PO4)5F] x 0.5H3O (denoted as AlPO-CJ20) with an Al/P ratio of 4:5 has been synthesized solvothermally by using 2-amino-2-methyl-1-propanol as the structure-directing agent. Its structure was determined by single-crystal X-ray diffraction analysis and further characterized by solid-state NMR techniques, including 27Al, 19F --> 27Al cross-polarization, and 31P magic angle spinning NMR. The alternation of Al-centered tetrahedra (AlO4 and AlO3F) and PO3(=O) tetrahedra gives rise to a new type of 4.6.16-net sheet. The inorganic sheets are stacked in an ABAB sequence along the [010] direction and further held together through strong H bonds between protonated template molecules and P=O groups in the inorganic layers. Except for Mu-4, AlPO-CJ20 is the second layered aluminophosphate with an Al/P ratio of 4:5, and it contains the largest pore opening of 16-rings in the known layered aluminophosphates. Furthermore, the coordination of Al and P of fluoroaluminophosphates is summarized. Crystal data: (C4H11NOH)3.5[Al4(PO4)5F] x 0.5H3O, monoclinic, C2/c (No. 15), a = 32.678(7) A, b = 12.956(3) A, c = 21.045(4) A, beta = 115.17(3) degrees, V = 8064(3) A3, Z = 8, R1 = 0.0837 [I > 2sigma(I)], and wR2 = 0.2428 (all data)." @default.
• W2046255364 created "2016-06-24" @default.
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• W2046255364 date "2007-01-01" @default.
• W2046255364 modified "2023-09-27" @default.
• W2046255364 title "Synthesis and Characterization of a New Layered Fluoroaluminophosphate (C₄H₁₁NOH)_3.5[Al₄(PO₄)₅F]·0.5H₃O with Extra-Large 16-Rings" @default.
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• W2046255364 doi "https://doi.org/10.1021/ic061362w" @default.
• W2046255364 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/17198421" @default.
• W2046255364 hasPublicationYear "2007" @default.
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