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- W2046372218 abstract "Die Struktur der Titelverbindung 1 wurde aus Diffraktometer-Einkristalldaten nach direkten Methoden bestimmt und für 1465 Reflexe zu einem R-Wert von 3.8% verfeinert. Die Verbindung kristallisiert monoklin in der Raumgruppe P21/c mit den Gitterkonstanten a = 7.958 Å, b = 5.222 Å, c = 19.297 Å, β = 101.24° Z = 4. Der PN-Sechsring ist schwach gewellt. Die endocyclischen PN-Abstände weisen signifikante Unterschiede auf (Einzelwerte: 1.551 ⃛1.586 Å, Mittelwert: 1.565 Å). Der Mittelwert der PF-Bindungslängen beträgt 1.521 Å, die Länge der PNAmin-Bindung ist 1.601 Å. Die Moleküle sind schichtartig über NH ⃛N-Wasserstoffbrücken verknüpft. The Crystal and Molecular Structure of 2-Amino 2,4,4,6,6,-pentafluoro-1,3,5,2λ5, 4λ5, 6λ5- triazatriphosphorine The crystal structure of the title compound 1 has been determined by direct methods from single crystal X-ray data and has been refined to R = 0.038 for 1465 reflections. The compound crystallizes in the monoclinic space group P21/c. The molecule forms a slightly puckered six-membered (PN)3 ring. The endocyclic PN bond lengths are significantly different (mean: 1.565 Å). The mean PF bond length is 1.521 Å, the PNamine bond length is 1.601 Å. The molecules are connected as layers through NH ⃛N hydrogen bonds." @default.
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- W2046372218 date "1975-09-01" @default.
- W2046372218 modified "2023-10-16" @default.
- W2046372218 title "Die Kristall- und Molekülstruktur von 2-Amino-2,4,4,6,6-pentafluor-1,3,5,2λ5,4λ5,6λ5-triazatriphosphorin" @default.
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- W2046372218 doi "https://doi.org/10.1002/cber.19751080913" @default.
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