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- W2046417344 abstract "Direct mercury (Hg) speciation was assessed for soil samples with a Hg concentration ranging from 7 up to 240 mg kg(-1). Hg chemical forms were identified and quantified by sequential extractions and bulk- and micro-analytical techniques exploiting synchrotron generated X-rays. In particular, microspectroscopic techniques such as mu-XRF, mu-XRD and mu-XANES were necessary to solve bulk Hg speciation, in both soil fractions <2 mm and <2 microm. The main Hg-species found in the soil samples were metacinnabar (beta-HgS), cinnabar (alpha-HgS), corderoite (Hg(3)S(2)Cl(2)), and an amorphous phase containing Hg bound to chlorine and sulfur. The amount of metacinnabar and amorphous phases increased in the fraction <2 microm. No interaction among Hg-species and soil components was observed. All the observed Hg-species originated from the slow weathering of an inert Hg-containing waste material (K106, U.S. EPA) dumped in the area several years ago, which is changing into a relatively more dangerous source of pollution." @default.
- W2046417344 created "2016-06-24" @default.
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- W2046417344 date "2010-08-01" @default.
- W2046417344 modified "2023-10-16" @default.
- W2046417344 title "Solving mercury (Hg) speciation in soil samples by synchrotron X-ray microspectroscopic techniques" @default.
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- W2046417344 doi "https://doi.org/10.1016/j.envpol.2010.04.016" @default.
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