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- W2046495384 abstract "Abstract The usefulness of terbium-sensitized luminescence for the determination of total phthalate esters in water samples is studied. A simple and fast method is described for this purpose, which could be used for screening purposes. After alkaline hydrolysis of phthalate esters, a luminescent chelate between terbium(III) and phthalate is formed. Luminescence measurements are obtained at λ ex 240 nm and λ em 545 nm by using the time-resolved mode of the instrument. Linear calibration graphs were obtained in the range 0.15–72 µM for dimethyl-, diethyl- and dibutylphthalate esters, and in the range 0.21–18 µM for bis(2-ethylhexyl)phthalate ester. The relative standard deviation was lower than 1.5%. The method was applied to the determination of total phthalates in drinking, well and river water samples. Solid-phase microextraction was used to avoid the loss of sensitivity in the analysis of water samples by dilution. Analytical recoveries ranged from 91.5 to 102.0%." @default.
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- W2046495384 date "2003-01-05" @default.
- W2046495384 modified "2023-09-26" @default.
- W2046495384 title "Application of Time-Resolved Luminescence Methodology to the Determination of Phthalate Esters" @default.
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- W2046495384 doi "https://doi.org/10.1081/al-120019259" @default.
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