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• W2046575509 abstract "Abstract Treatment of the ligand 1,5‐bis(3,5‐dimethyl‐1‐pyrazolyl)‐3‐thiapentane (bdtp) with [PdCl 2 (CH 3 CN) 2 ] led to a [PdCl 2 (bdtp)] complex. Subsequent treatment of this complex with AgBF 4 gave [PdCl(bdtp)](BF 4 ). These Pd II complexes were characterised by elemental analysis, conductivity measurements, IR spectroscopy, and 1 H and 13 C NMR spectroscopy. Complex [PdCl 2 (bdtp)] was again obtained when the complex [PdCl(bdtp)](BF 4 ) was heated under reflux in a solution of NEt 4 Cl in CH 2 Cl 2 /MeOH (1:1). Ligand bdtp in complexes 1 and 2 exhibited a hemilabile character. The X‐ray structure of the complex [PdCl(bdtp)](BF 4 ) was determined. The metal atom is tricoordinated by the two azine nitrogen atoms and one thioether sulfur atom of the thioether‐pyrazole ligand, its coordination (distorted square planar) being completed with one chloride ion. (© Wiley‐VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, Germany, 2003)" @default.
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• W2046575509 date "2003-10-28" @default.
• W2046575509 modified "2023-10-18" @default.
• W2046575509 title "Synthesis of New Pd^II Complexes Containing a Thioether‐Pyrazole Hemilabile Ligand − Structural Analysis by ¹H, ¹³C NMR Spectroscopy and Crystal Structure of [PdCl(bdtp)]BF₄ [bdtp = 1,5‐Bis(3,5‐dimethyl‐1‐pyrazolyl)‐3‐thiapentane]" @default.
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• W2046575509 doi "https://doi.org/10.1002/ejic.200300235" @default.
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