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- W2046599944 abstract "Abstract The reaction of nickelocene with BrMgR, where R=CH 2 CH(CH 3 )C 6 H 5 , C 2 H 5 , (CH 2 ) 7 CH 3 and CH 2 CH 2 CH 3 , have been studied. It was found that the presence of β -hydrogen in R did not cause the total splitting of the carbon–nickel bond but alkylidynetrinickel clusters were formed. It is the first example of the synthesis of alkylidynetrinickel clusters (NiCp) 3 CR′ from the organonickel species possessing β -hydrogen. Besides trinickel clusters, the following compounds were always formed in all the studied reactions: (NiCp) 4 H 2 , (NiCp) 6 , CpNi( η 3 -C 5 H 7 ) and (NiCp) 2 ( μ -C 5 H 6 ). The structure of (NiCp) 3 CCH(CH 3 )Ph has been determined by a single-crystal X-ray diffraction study." @default.
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- W2046599944 date "1998-01-01" @default.
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- W2046599944 title "Reactions of nickelocene with lithium and magnesium alkyls containing β-hydrogen atoms1Dedicated to Professor Ken Wade on the occasion of his 65th birthday in recognition of his outstanding contributions to organometallic chemistry.1" @default.
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- W2046599944 doi "https://doi.org/10.1016/s0022-328x(97)00179-4" @default.
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