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- W2046646764 abstract "Abstract The pseudo C 2 ‐symmetrical diketone 22 was efficiently constructed from furan‐3,4‐dimethanol ( 7 ) using a two‐directional route featuring a double asymmetric dihydroxylation. Acidic hydrolysis of the cyclopentylidene acetals of 22 triggered a selective cyclization of the resulting hexaol diketone to generate the 2,8‐dioxabicyclo[3.2.1]octane core of the zaragozic acids/squalestatins. Chemoselective oxidative cleavage of a superfluous two‐carbon appendage and further functional group manipulations yielded the enantiomerically pure triester 30 , which offers itself as a general heterobicyclic building block for naturally occurring zaragozic acids/squalestatins and unnatural analogues." @default.
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- W2046646764 date "2009-09-01" @default.
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- W2046646764 title "A Symmetry-Based Synthesis of the Heterobicyclic Core of the Zaragozic Acids/Squalestatins" @default.
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