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- W2046693773 abstract "Reactions of terminal chloroaminophosphido complexes with Co 2 (CO) 8 have been examined. The ruthenium phosphido complexes [Cp*Ru(CO) 2 {P(Cl)TMP}] (1a) and [CpRu(CO) 2 {P(Cl)TMP}] (1b) (TMP = 2,2,6,6-tetramethylpiperidinyl) react with Co 2 (CO) 8 to form the cobalt cluster [Co 4 (CO) 7 (µ-CO) 3 {µ 3 -P(TMP)}] (2) with complete transfer of the phosphinidene unit to cobalt. In contrast, the phosphido complex [Cp*Ru(CO) 2 {P(Cl)N-i-Pr 2 }] (1c) affords the spiked-triangular cluster [Cp*RuCo 3 (CO) 8 (µ-CO) 2 (µ 3 -PN-i-Pr 2 )] (3), which retains the Cp*Ru unit upon reaction with Co 2 (CO) 8 . The molybdenum phosphido complex [CpMo(CO) 2 {P(Cl)TMP}] (4) reacts with Co 2 (CO) 8 to form cluster 2, while [Cp*Mo(CO) 3 {P(Cl)N-i-Pr 2 }] (5) generates the mixed metal tetrahedral cluster [Cp*MoCo 3 (CO) 5 (µ-CO) 4 (µ 3 -PN-i-Pr 2 )] (6). Key words: phosphido, phosphinidene, cobalt, ruthenium, molybdenum, cluster." @default.
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- W2046693773 date "2003-11-01" @default.
- W2046693773 modified "2023-09-25" @default.
- W2046693773 title "The formation of mixed metal aminophosphinidene clusters via reactions of terminal chloroaminophosphido complexes with Co<sub>2</sub>(CO)<sub>8</sub>" @default.
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- W2046693773 doi "https://doi.org/10.1139/v03-103" @default.
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