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- W2046807780 abstract "The synthesis and characterization of a family of potassium silanethiolates is described. [( t BuO)3SiSK]6[THF]2· 2THF ( 1 ), {[( t BuO)3SiS]2K2} n ( 2 ), and [( t BuO)3SiSK]4[H2O]4· C6H6 ( 3 ) were synthesized by treatment of ( t BuO)3SiSH with potassium metal in various solvents. The target molecules were characterized by single crystal X-ray crystallography. Compounds 1 , 2 , and 3 form hexameric, polymeric, and tetrameric units correspondingly, in the solid state. [( t BuO)3SiSK]6[THF]2· 2THF contains three, differently coordinated potassium ions and crystallizes in the space group P21/c, a = 15.227(4), b = 14.650(5), c = 32.067(9) Å, β = 117.001(18)°, V = 6374(3) Å3. {[( t BuO)3SiS]2K2} n crystallizes in the space group P-1, a = 11.6305(14), b = 13.348(3), c = 13.531(4) Å, α = 67.27(2)°, β = 76.064(16)°, γ = 88.706(14)°, V = 1874.6(8) Å3. [( t BuO)3SiSK]4[H2O]4· C6H6 crystallizes in the space group P-4b2, a = 20.854(3), b = 20.854(3), c = 9.283(2) Å, α = β = γ = 90°, V = 4037,1(12) Å3." @default.
- W2046807780 created "2016-06-24" @default.
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- W2046807780 date "2009-06-06" @default.
- W2046807780 modified "2023-09-27" @default.
- W2046807780 title "Potassium Tri-tert-butoxysilanethiolates: Synthesis, Properties, and Crystal and Molecular Structures of [( t BuO)3SiSK]6[THF]2· 2THF, {[( t BuO)3SiS]2K2} n , and [( t BuO)3SiSK]4[H2O]4· C6H6" @default.
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- W2046807780 doi "https://doi.org/10.1080/10426500902947674" @default.
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