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• W2047016834 abstract "The infrared and Raman spectra of four polymorphic phases (α, α1, γ and γ1) of erucic acid (cis-13-docosenoic acid) and those of two polymorphic phases (α and γ) of palmitoleic acid (cis-9-hexadecenoic acid) were investigated. The γ and γ1 phases of erucic acid were analyzed on the basis of crystal structures determined by us. There were large spectral differences between γ and γ1 phases, which could be ascribed to the differences in the conformation of cis-olefin groups and the subcell structure. Two types of reversible solid state phase transitions (γ→α and γ1→α1 transitions) were followed by the infrared and Raman spectra. It was concluded that the mechanism of the γ→α phase transition of erucic and palmitoleic acids is essentially the same as that of oleic acid previously reported by us [J. Phys. Chem. 90, 6371 (1986)], i.e. this phase transition is of order-disorder type accompanied by a conformational disordering at the methyl-terminal chain. Spectral changes on the γ1→α1 transition suggested that a similar structural change took place during this transition but there were large structural differences between α and α1." @default.
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• W2047016834 date "1994-07-01" @default.
• W2047016834 modified "2023-10-16" @default.
• W2047016834 title "Vibrational spectroscopic study on polymorphism of erucic acid and palmitoleic acid: γ1→α1 and γ→α reversible solid state phase transitions" @default.
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• W2047016834 doi "https://doi.org/10.1016/0584-8539(94)e0069-m" @default.
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