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• W2047100152 abstract "Dextran fractions from NRRL strains Leuconostoc mesenteroides B-742, B-1299, B-1355, and B-1501, Streptobacterium dextranicum B-1254, Streptococcus sp. B-1526, and also the native dextrans from L. mesenteroides B-1142, B-1191, B-1402, and L. dextranicum B-1420 were examined in aqueous solution at 90° by Fourier-transform, 1H-n.m.r. spectroscopy. Branching of dextrans through the 2,6-, 3,6-, and 4,6-di-O-substituted α-d-glucopyranosyl residues was correlated to changes in spectral patterns. The major, spectral differences for these dextrans were in the anomeric (4-6-p.p.m.) region. In general, the degree of branching of a dextran can be determined by comparing anomeric-peak integrals; however, the integrals of the displaced, nonlinear, anomeric resonances are also dependent on the type of branching residues present in the dextran. Although the 1H-n.m.r. resonances for the anomeric region identify the presence of non-6-mono-O-substituted α-d-glucopyranosyl residues, these additional resonances provide little discrimination between other residue types, the exception being the 2,6-di-O-substituted residue, which has a clearly displaced resonance. Techniques for the suppression of the interfering resonance of deuterium hydroxide are also discussed." @default.
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• W2047100152 date "1979-09-01" @default.
• W2047100152 modified "2023-10-14" @default.
• W2047100152 title "Correlation of the structure of dextrans to their 1H-n.m.r. Spectra" @default.
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• W2047100152 doi "https://doi.org/10.1016/s0008-6215(00)84766-7" @default.
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