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- W2047162219 endingPage "6985" @default.
- W2047162219 startingPage "6972" @default.
- W2047162219 abstract "Four 1,2,7-trioxa-spiro[5.5]undecanes and two 1,6,7-trioxa-spiro[4.5]decanes were synthesized using the hydrogen peroxide in UHP (urea–H2O2 complex) as the source of the peroxy bond. Incorporation of H2O2 into the organic molecular framework was facilitated by the potential to form a five- or six memberd cyclic hemiketal. Saturation of the double bond in a substituted γ-keto-butenal, a step required in all the syntheses, was achieved in one case with NaI/concd HCl at low temperature without cleaving the TBS protecting group or causing excessive side reactions as observed at ambient temperature. All these peroxides showed in vitro antimalarial activity comparable to that of natural peroxyplakoric acids and the known analogues." @default.
- W2047162219 created "2016-06-24" @default.
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- W2047162219 date "2009-08-01" @default.
- W2047162219 modified "2023-10-09" @default.
- W2047162219 title "Synthesis and in vitro antimalarial activity of spiro-analogues of peroxyplakoric acids" @default.
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- W2047162219 doi "https://doi.org/10.1016/j.tet.2009.06.050" @default.
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