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• W2047264830 abstract "Three novel metal polyphosphides, α-SrP3, BaP8, and LaP5, were prepared in BN crucibles by the reaction of the respective stoichiometric mixtures under a high pressure of 3 GPa at 950–1000°C. Their crystal structures were determined from single-crystal X-ray data (α-SrP3: space group C2/m, a=9.199(6) Å, b=7.288(3) Å, c=5.690(3) Å, β=113.45(4)°, Z=4, R1/wR2=0.0684/0.1180 for 471 observed reflections and 22 variables; BaP8: space group P−1, a=6.762(2) Å, b=7.233(2) Å, c=8.567(2) Å, α=86.32(2)°, β=84.31(2)°, γ=70.40(2)°, Z=2, R1/wR2=0.0476/0.1255 for 2702 observed reflections and 82 variables; LaP5: space group P21/m, a=4.885(1) Å, b=9.673(3) Å, c=5.577(2) Å, β=105.32(2)°, Z=2, R1/wR2=0.0391/0.1034 for 1272 observed reflections and 31 variables). α-SrP3 is isostructural with SrAs3 and the crystal structure consists of two-dimensional puckered polyanionic layers ∞2[P3]2− that stack along the c-axis yielding channels occupied by Sr2+ counterions. BaP8 crystallizes in a new structure type which contains a three-dimensional infinite polyanionic framework ∞3[P3]2−, with large channels hosting the barium cations. LaP5 is a layered compound containing ∞2[P5]3− polyanionic layers separated by La3+ ions. All three compounds exhibit expected diamagnetic behaviors." @default.
• W2047264830 created "2016-06-24" @default.
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• W2047264830 date "2003-07-01" @default.
• W2047264830 modified "2023-10-02" @default.
• W2047264830 title "High-pressure synthesis and structural characterization of three new polyphosphides, α-SrP3, BaP8, and LaP5" @default.
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• W2047264830 doi "https://doi.org/10.1016/s0022-4596(03)00142-7" @default.
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