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- W2047295572 abstract "An unmodified split/splitless inlet system using forward-pressure controlled pneumatics was operated in splitless injection mode with several inlet liners under a range of septum purge flow rates. The relative recovery (discrimination) of hydrocarbons ranging from n-C8 to n-C20 depended strongly upon the injected sample volume with open-ended liners at high septum purge flow rates of e.g. 50 mL/min. Little or no discrimination was observed at septum purge flows of 2–3 mL/min. The same inlet was also operated in a back-pressure regulated configuration that produced mass discrimination similar to that observed with the higher septum purge flows in the forward-pressure configuration. An inlet liner with a restricted inlet and outlet gave mass-discrimination levels independent of septum purge flow rate, but in the reverse sense of that observed with open-ended liners. Preferential volatile-component losses out of the inlet liner to the septum purge vent are principally responsible for the observed mass discrimination with openended liners, while mass-dependent losses with doubly-restricted liners seem due to slow sample evaporation." @default.
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- W2047295572 date "1993-04-01" @default.
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- W2047295572 title "The effects of inlet liner configuration and septum purge flow rate on discrimination in splitless injection" @default.
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- W2047295572 doi "https://doi.org/10.1002/jhrc.1240160409" @default.
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