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• W2047360557 startingPage "4099" @default.
• W2047360557 abstract "A series of [Fe4X4(YR)4]2− (X,Y=S and Se; R=n-C12H25 and C6H4-p-t-Bu) were prepared as n-Bu4N+ salts. In aqueous Triton X-100 micellar solutions, only the reduced forms of [Fe4X4(YR)4]2− (X,Y=S and Se; R=n-C12H25 and C6H4-p-t-Bu) undergo protonation reactions at the sulfur or selenium atom of the Fe4X4 (X=S and Se) core to exist as an equilibrium mixture of the protonated and unprotonated clusters. On the other hand, not only the oxidized but also the reduced forms of [Fe4X4(YC6H4-p-t-Bu)4]2− (X,Y=S and Se) undergo protonation reactions in aqueous poly[2-(dimethylamino)hexanamide] (PDACA) solutions. The pKox values of [Fe4X4(YC6H4-p-t-Bu)4]2− (X,Y=S and Se) vary depending on the terminal thiolate and selenolate ligands; 5.9 for Y=S and 6.8 for Y=Se, whereas the pKred values of [Fe4X4(YC6H4-p-t-Bu)4]3− are controlled by the core sulfur and selenium; 8.8 for X=S and 7.3 for X=Se. Such characteristic pKox and pKred values suggest that the protonation takes place at the terminal sulfur or selenium atom of the oxidized clusters [Fe4X4(YC6H4-p-t-Bu)4]2− (X,Y=S and Se), while it occurs at the sulfur or selenium atom of the Fe4X4 core of the reduced clusters [Fe4X4(YC6H4-p-t-Bu)4]3− (X,Y=S and Se)." @default.
• W2047360557 created "2016-06-24" @default.
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• W2047360557 date "1988-11-01" @default.
• W2047360557 modified "2023-10-14" @default.
• W2047360557 title "Redox-Linked Protonation of [Fe₄X₄(YR)₄]²⁻(X,Y=S and Se; R=<i>n</i>-C₁₂H₂₅and C₆H₄-<i>p</i>-<i>t</i>-Bu) in Aqueous Solutions" @default.
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• W2047360557 doi "https://doi.org/10.1246/bcsj.61.4099" @default.
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