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• W2047568802 abstract "A multifunctional additive, bis(diisopropyl) thiophosphoryl diisopropyl disulfide (DIPDIS), was melted in the presence of quaternary ammonium-modified montmorillonite clay and incorporated into an ethylene propylene diene terpolymer (EPDM) rubber matrix as a nanofiller to prepare EPDM rubber nanocomposites. The finer dispersion of the organoclay (OC) in the rubber matrix was observed when the OC was preintercalated by DIPDIS using the propping-open procedure. X-ray diffraction (XRD) results showed that the silicate layers of the OC were successfully preintercalated by the DIPDIS; that is, the basal spacing of clay galleries was expanded from 2.98 to 3.76 nm. Because of the larger interlayer distance, as evidenced by XRD studies, the delamination process was facilitated through the easy intercalation of macromolecular rubber chains, which was reflected in various properties, such as the stress–strain behavior, thermal stability, dynamic mechanical properties and swelling properties. XRD studies and transmission electron microscopy directly supported the effective filler dispersion in the non-polar EPDM rubber matrix. The present paper focuses on the utilization of the combination of low molecular weight vulcanizing accelerator with clay minerals for creating new rubber material with enhanced performance and properties. Gradual expansion of the interlayer space of the clay minerals was carried out by disteraylammonium compound followed by bis(diisopropyl) thiophosphoryl disulfide. Therefore, such expanded clay minerals facilitate easier penetration of the macromolecular rubber chains into the interlayer space of the clay minerals." @default.
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• W2047568802 date "2011-01-26" @default.
• W2047568802 modified "2023-10-18" @default.
• W2047568802 title "Preintercalation of an organic accelerator into nanogalleries and preparation of ethylene propylene diene terpolymer rubber–clay nanocomposites" @default.
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• W2047568802 doi "https://doi.org/10.1038/pj.2010.132" @default.
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