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- W2047573797 abstract "A crystalline mixed ester, 6-O-acetyl-2,3,4-tri-O-[(+)-3-methylvaleryl]-β-d-glucopyranose, was obtained from Turkish tobacco by column chromatography and liquid-liquid partitions of a hexane extract. Saponification of the ester gave glucose, identified by paper chromatography, and acetic and 3-methylpentanoic (3-methylvaleric) acids, identified by gas chromatography and by the formation of their p-phenylphenacyl esters. Exhaustive methylation of the mixed ester, followed by saponification of the methylated ester gave methyl β-d-glucopyranoside. Confirmation of the structure of the ester was provided by its synthesis from d-glucose, (+)-3-methylvaleric acid, and acidic acid in 43% yield." @default.
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- W2047573797 date "1970-04-01" @default.
- W2047573797 modified "2023-09-26" @default.
- W2047573797 title "The isolation of 6-O-acetyl-2,3,4-tri-O-[(+)-3-methylvaleryl]-β-d-glucopyranose from tobacco" @default.
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- W2047573797 doi "https://doi.org/10.1016/s0008-6215(00)84888-0" @default.
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