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- W2047713636 abstract "Recently, it has been shown that the DEPT sequence may be used to provide separate methyl, methylene, and methine subspectra and preliminary results have indicated it is quite an accurate sequence for this purpose. Here, the errors involved in using DEPT over the normal range of aliphatic and aromatic 1J13C-1H, values are assessed by analyzing DEPT with variable time delay periods using the Heisenberg quantum picture approach. The limitations of the sequence when used across the whole range of organic compounds is discussed. An experimental approach to setting up and using the sequence is described. The possibility of improving the sequence with additional phase-alternation schemes or composite pulses, for example, is explored. The editing of a 13C spectrum is completed by generation of a spectrum containing unprotonated (quaternary) carbons only. The theoretical basis of the pulse sequence used for this purpose is described and errors are assessed." @default.
- W2047713636 created "2016-06-24" @default.
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- W2047713636 date "1983-06-01" @default.
- W2047713636 modified "2023-10-10" @default.
- W2047713636 title "Complete accurate editing of decoupled 13C spectra using DEPT and a quaternary-only sequence" @default.
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- W2047713636 doi "https://doi.org/10.1016/0022-2364(83)90032-x" @default.
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