Matches in SemOpenAlex for { <https://semopenalex.org/work/W2047733620> ?p ?o ?g. }
Showing items 1 to 92 of
92
with 100 items per page.
- W2047733620 endingPage "226" @default.
- W2047733620 startingPage "219" @default.
- W2047733620 abstract "A sensitive and selective liquid chromatography-tandem mass spectrometry (LC-MS-MS) method for confirmatory analysis of 17beta-boldenone (17beta-BOL), 17alpha-boldenone (17alpha-BOL) and androsta-1,4-diene-3,17-dione (ADD) in bovine urine was developed. [2H(2)]17beta-Testosterone (17beta-T-d(2)) was used as the internal standard. Sample preparation involved enzymatic hydrolysis and purification on a C(18) solid-phase extraction column. Chromatographic separation of the analytes was obtained using an RP-C(18) HPLC column. LC-MS-MS detection was carried out with an atmospheric pressure chemical ionisation (APCI) source equipped with a heated nebulizer (HN) interface operating in the positive ion mode. For unambiguous hormone confirmation, three analyte precursor-product ion combinations were monitored during multiple-reaction monitoring (MRM) LC-MS-MS analysis. Overall recovery (%), repeatability (relative standard deviations, RSD, %) and within-laboratory reproducibility (RSD, %) ranged from 92.2 to 97.7%, from 6.50 to 2.94% and from 13.50 to 5.04%, respectively, for all analytes. The limit of quantification in bovine urine was 0.20 ng ml(-1) for 17beta-BOL and ADD and 0.50 ng ml(-1) for 17alpha-BOL. The validated method was successfully applied for determination of 17beta-BOL, 17alpha-BOL and ADD in a large number of bovine urine samples collected within the national Official Residue Control Program." @default.
- W2047733620 created "2016-06-24" @default.
- W2047733620 creator A5038315447 @default.
- W2047733620 creator A5070647179 @default.
- W2047733620 creator A5071513520 @default.
- W2047733620 creator A5080899906 @default.
- W2047733620 creator A5087905057 @default.
- W2047733620 date "2003-06-01" @default.
- W2047733620 modified "2023-10-01" @default.
- W2047733620 title "Confirmatory analysis of 17β-boldenone, 17α-boldenone and androsta-1,4-diene-3,17-dione in bovine urine by liquid chromatography–tandem mass spectrometry" @default.
- W2047733620 cites W1964721735 @default.
- W2047733620 cites W1965937649 @default.
- W2047733620 cites W1976489916 @default.
- W2047733620 cites W1977291403 @default.
- W2047733620 cites W1985428025 @default.
- W2047733620 cites W1986458330 @default.
- W2047733620 cites W1999535865 @default.
- W2047733620 cites W2014324256 @default.
- W2047733620 cites W2025557071 @default.
- W2047733620 cites W2040653752 @default.
- W2047733620 cites W2041761277 @default.
- W2047733620 cites W2046822780 @default.
- W2047733620 cites W2085596677 @default.
- W2047733620 cites W2086799306 @default.
- W2047733620 cites W2087185974 @default.
- W2047733620 cites W2121334549 @default.
- W2047733620 doi "https://doi.org/10.1016/s1570-0232(03)00072-2" @default.
- W2047733620 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/12742113" @default.
- W2047733620 hasPublicationYear "2003" @default.
- W2047733620 type Work @default.
- W2047733620 sameAs 2047733620 @default.
- W2047733620 citedByCount "38" @default.
- W2047733620 countsByYear W20477336202012 @default.
- W2047733620 countsByYear W20477336202013 @default.
- W2047733620 countsByYear W20477336202016 @default.
- W2047733620 countsByYear W20477336202018 @default.
- W2047733620 crossrefType "journal-article" @default.
- W2047733620 hasAuthorship W2047733620A5038315447 @default.
- W2047733620 hasAuthorship W2047733620A5070647179 @default.
- W2047733620 hasAuthorship W2047733620A5071513520 @default.
- W2047733620 hasAuthorship W2047733620A5080899906 @default.
- W2047733620 hasAuthorship W2047733620A5087905057 @default.
- W2047733620 hasConcept C10390740 @default.
- W2047733620 hasConcept C119128265 @default.
- W2047733620 hasConcept C145148216 @default.
- W2047733620 hasConcept C148065180 @default.
- W2047733620 hasConcept C154020017 @default.
- W2047733620 hasConcept C162356407 @default.
- W2047733620 hasConcept C178790620 @default.
- W2047733620 hasConcept C185592680 @default.
- W2047733620 hasConcept C198291218 @default.
- W2047733620 hasConcept C31827203 @default.
- W2047733620 hasConcept C43617362 @default.
- W2047733620 hasConcept C51884965 @default.
- W2047733620 hasConcept C64489805 @default.
- W2047733620 hasConcept C71043704 @default.
- W2047733620 hasConceptScore W2047733620C10390740 @default.
- W2047733620 hasConceptScore W2047733620C119128265 @default.
- W2047733620 hasConceptScore W2047733620C145148216 @default.
- W2047733620 hasConceptScore W2047733620C148065180 @default.
- W2047733620 hasConceptScore W2047733620C154020017 @default.
- W2047733620 hasConceptScore W2047733620C162356407 @default.
- W2047733620 hasConceptScore W2047733620C178790620 @default.
- W2047733620 hasConceptScore W2047733620C185592680 @default.
- W2047733620 hasConceptScore W2047733620C198291218 @default.
- W2047733620 hasConceptScore W2047733620C31827203 @default.
- W2047733620 hasConceptScore W2047733620C43617362 @default.
- W2047733620 hasConceptScore W2047733620C51884965 @default.
- W2047733620 hasConceptScore W2047733620C64489805 @default.
- W2047733620 hasConceptScore W2047733620C71043704 @default.
- W2047733620 hasIssue "2" @default.
- W2047733620 hasLocation W20477336201 @default.
- W2047733620 hasLocation W20477336202 @default.
- W2047733620 hasOpenAccess W2047733620 @default.
- W2047733620 hasPrimaryLocation W20477336201 @default.
- W2047733620 hasRelatedWork W1985186853 @default.
- W2047733620 hasRelatedWork W1998754189 @default.
- W2047733620 hasRelatedWork W2003020830 @default.
- W2047733620 hasRelatedWork W2035321010 @default.
- W2047733620 hasRelatedWork W2044145238 @default.
- W2047733620 hasRelatedWork W2169361849 @default.
- W2047733620 hasRelatedWork W2319580498 @default.
- W2047733620 hasRelatedWork W2567898155 @default.
- W2047733620 hasRelatedWork W28056001 @default.
- W2047733620 hasRelatedWork W2953950333 @default.
- W2047733620 hasVolume "789" @default.
- W2047733620 isParatext "false" @default.
- W2047733620 isRetracted "false" @default.
- W2047733620 magId "2047733620" @default.
- W2047733620 workType "article" @default.