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- W2047970606 abstract "A synthetic methodology for the synthesis of 13,14-seco-steroids with substituents at C-14 and C-17 is described. The approach involves Grob fragmentation of 14β-hydroxy-17β-tosylates, hydroboration–oxidation of the intermediate Δ13(17)-olefin, and hydride reduction of the 14-ketone. An unambiguous structural assignment of (13R,14S,17S)-14,17-diacetoxy-3-methoxy-7α-methyl-13,14-secoestra-1,3,5(10)-triene was determined by X-ray analysis." @default.
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- W2047970606 date "2004-07-01" @default.
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- W2047970606 title "The synthesis of functionalized 13,14-seco-steroids via Grob fragmentation" @default.
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- W2047970606 doi "https://doi.org/10.1016/j.steroids.2004.04.009" @default.
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