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- W2048049480 abstract "An investigation of the Nb–Tl–O system has allowed the synthesis of a new phase, Tl8Nb27.2O72. This phase is structurally and chemically close to a Tl–Nb–O phase previously described as a builtup hexagonal bronze witha≈7.4 Å,b≈13 Å,c≈7.6 Å, and an orthorhombic C-type lattice. The electron diffraction study evidences a doubling of thecparameter with regard to the C cell, resulting in an orthorhombic I-type lattice with, in addition, the observation of a second superstructure and twinned microdomains. A structural determination of the mean orthorhombic I-type cell was successfully carried out by combining energy dispersion spectroscopy (EDS) and single-crystal XRD studies and leads toa=7.534(7) Å,b=12.992(12) Å,c=15.555(12) Å,Z=8, space groupIm2m,R=0.097, andRw=0.099 from 995 independent reflections. A chemical formula for this thallium niobate, Tl8Nb27.2O72, consistent with EDS results, was deduced by structure refinement. HREM investigations on this phase clearly show irregular occupancy of the supplementary crystallographic positions by niobium atoms together with a monocommensurate modulated structure and twinned microdomains." @default.
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- W2048049480 date "1998-02-01" @default.
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- W2048049480 title "Synthesis and Crystal Structure Determination of Tl8Nb27.2O72Using TEM and Single-Crystal X-Ray Diffraction" @default.
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- W2048049480 doi "https://doi.org/10.1006/jssc.1997.7638" @default.
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