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• W2048280003 abstract "Thermal and microstructural characterization of the TeO2–WO3 binary system was accomplished by applying differential thermal analysis (DTA), X-ray diffraction (XRD) and scanning electron microscopy (SEM) techniques. Different compositions of the (1 − x)TeO2–xWO3 system, where x varies between 0.02 and 0.80 in molar ratio were studied. The samples were prepared by melting high purity powder mixtures of TeO2 and WO3 in a platinum crucible with a closed lid at 750 °C for 30 min and quenching in water bath. The glass forming range of the binary system was detected as 0.04 ≤ x ≤ 0.35 in molar ratio. As-cast samples were heat-treated above the crystallization peak temperatures at 550 °C for 24 h to obtain thermal stability and the phase stability of the binary system was investigated by performing systematical thermal, phase and microstructural characterizations with the heat-treated samples. The eutectic reaction of the binary system was detected at 617 ± 3 °C, the endothermic reaction indicating the phase transformation reaction of WO3 from orthorhombic to tetragonal was determined at 743 ± 1 °C. α-TeO2 and orthorhombic WO3 crystalline phases were found to be present in the final structure when the total crystallization was achieved. Microstructural characterization of the TeO2–WO3 system was realized for a wide compositional range for the first time in the literature." @default.
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• W2048280003 date "2011-05-01" @default.
• W2048280003 modified "2023-09-26" @default.
• W2048280003 title "Investigation on thermal and microstructural characterization of the TeO2–WO3 system" @default.
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• W2048280003 doi "https://doi.org/10.1016/j.jallcom.2011.02.109" @default.
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