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- W2048334491 abstract "Effects of the crystallization temperature on the crystal structure and its melting behavior of poly (l-lactic acid) (PLLA) have been investigated by means of wide-angle (WAXS) and small-angle (SAXS) X-ray scattering, optical microscopy, and differential scanning calorimetory (DSC). PLLA was found to crystallize as the α form when the crystallization temperature Tc was higher than 120 °C, while significant change in lattice parameters was seen for Tc's below 120 °C. The ratio of the a- and b-axis lengths begins to decrease with Tc below 120 °C and is 31/2 below 90 °C, which suggests a new crystalline form with hexagonal packing, namely, the α‘ form. The possible reason for α‘ formation is discussed. High-temperature WAXS and SAXS measurements showed that α‘ crystal transforms into ordered a form during heating. The transition takes place at 150 °C without a decrease in scattering intensity and without heating rate dependence. The mechanism for the transition is discussed." @default.
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- W2048334491 date "2007-11-22" @default.
- W2048334491 modified "2023-09-30" @default.
- W2048334491 title "Crystallization and Melting Behavior of Poly (<scp>l</scp>-lactic Acid)" @default.
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- W2048334491 doi "https://doi.org/10.1021/ma070082c" @default.
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