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• W2048432823 abstract "Well shaped single crystals of the equiatomic germanides YbPdGe and YbPtGe were synthesized from the elements using the Bridgman technique. The samples were investigated by X-ray powder and single crystal diffraction: YbAuSn type, Imm2, a = 433.4(2), b = 2050.6(6), c = 752.6(2) pm, wR2 = 0.0723, 1551 F2 values, 58 variables for YbPdGe and TiNiSi type, Pnma, a = 686.32(9), b = 430.47(9), c = 751.02(8) pm, wR2 = 0.0543, 379 F2 values, 20 variables for YbPtGe. Both germanides crystallize with different superstructure variants of the KHg2 type, resulting from different stacking of the puckered Pd3Ge3 and Pt3Ge3 hexagons. While only Pt–Ge interactions occur in the [PtGe] polyanionic network of YbPtGe, weak interlayer Pd–Pd (297 pm) and Ge–Ge (275 pm) interactions occur in YbPdGe. The crystal chemical peculiarities are discussed in the light of the different superstructure formed." @default.
• W2048432823 created "2016-06-24" @default.
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• W2048432823 date "2008-07-01" @default.
• W2048432823 modified "2023-09-25" @default.
• W2048432823 title "Bridgman Crystal Growth and Structure Refinement of YbPdGe and YbPtGe – Two Different Superstructures of the KHg2 Type" @default.
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• W2048432823 doi "https://doi.org/10.1002/zaac.200800036" @default.
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