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- W2048644159 abstract "Two unknown impurities in linezolid bulk drug at levels below 0.1% (ranging from 0.05 to 0.1%) were detected by a simple isocratic reverse phase high performance liquid chromatography (HPLC). These impurities were isolated from crude sample of linezolid using reverse phase preparative HPLC. Based on the spectroscopic data (IR, NMR and MS) the structures of the impurities were characterized as (S)-N-[[-(3-(3-fluoro-4-(4-morpholinyl)phenyl]-2-oxo-5-oxazolidinyl]methyl] acetate(I) and (S)-N-[[-(3-(3-fluoro-4-(4-morpholinyl)phenyl]-2-oxo-5-oxazolidinyl]methyl] chloride(II). The synthesis from an unambiguous route and the formation of impurities was discussed." @default.
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- W2048644159 date "2002-10-01" @default.
- W2048644159 modified "2023-09-23" @default.
- W2048644159 title "Isolation and characterization of process-related impurities in linezolid" @default.
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- W2048644159 doi "https://doi.org/10.1016/s0731-7085(02)00353-9" @default.
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