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• W2048645199 abstract "Bismuth vanadates with multiple morphologies and/or porous structures were prepared using the alcoho-hydrothermal strategy with bismuth nitrate and ammonium metavanadate as metal source, NaOH as pH adjustor, ethanol and ethylene glycol as solvent, and/or dodecylamine (DA), oleylamine (OL) or oleic acid (OA) as surfactant. The materials were characterized by means of the XRD, Raman, TGA/DSC, FT-IR, BET, SEM, TEM, XPS, and UV–vis techniques. The photocatalytic performance of the as-obtained samples was evaluated for the degradation of phenol in the presence of a small amount of H2O2 under visible-light irradiation, and the effect of phenol concentration on the photocatalytic activity was also examined. It is found that the surfactant and pH value had a significant influence on the particle morphology and even the crystalline structure of the product. Porous olive-like monoclinic BiVO4 samples could be prepared with DA, OL or OA as surfactant at pH = 1.5 or 3.0 and alcoho-hydrothermal temperature = 100 °C. With DA as surfactant at an alcoho-hydrothermal temperature of 100 °C, short-rod-like monoclinic BiVO4 and porous sheet-layered spherical orthorhombic Bi4V2O11 were obtained when the pH value of the precursor solution was raised to 7.0 and 11.0, respectively. Among the BiVO4 samples, the porous olive-like one with a surface area of 12.7 m2/g exhibited the best visible-light-driven photocatalytic performance for phenol degradation. It is concluded that the excellent photocatalytic activity of the porous olive-like BiVO4 sample was associated with its higher surface area and surface oxygen vacancy density, porous structure, lower bandgap energy, and unique morphology." @default.
• W2048645199 created "2016-06-24" @default.
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• W2048645199 date "2011-06-01" @default.
• W2048645199 modified "2023-10-10" @default.
• W2048645199 title "Porous olive-like BiVO4: Alcoho-hydrothermal preparation and excellent visible-light-driven photocatalytic performance for the degradation of phenol" @default.
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• W2048645199 doi "https://doi.org/10.1016/j.apcatb.2011.04.026" @default.
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