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- W2048742069 abstract "C10HtlN604Rb 4HzO is monoclinic, space group P21, with a=8.901 (3), b=6.455 (2), c= 15.379 (5),~, fl= 10543 (4) °, Z = 2. The structure was solved by the heavy-atom method and refined by full-matrix least-squares calculations to a final R of 0-050 for 1190 counter reflexions. The molecules exist in the N(9)-H tautomeric form. The molecular geometry is determined by the conformationally preferred internal hydrogen bond between N(12)-H of the ureidothreonine side chain and N(1) of purine, 2-693 A. The purine rings display approximately parallel, head-to-tail stacking with an interplanar spacing of about 3.2 ,~,. Rb is coordinated by one N and five O atoms. The water molecules form two hydrophilic zones in the crystal." @default.
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- W2048742069 date "1975-05-15" @default.
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- W2048742069 title "The structure of the rubidium salt of N-(purin-6-ylcarbamoyl)-L-threonine tetrahydrate, a hypermodified base in the anticodon loop of some tRNA's" @default.
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