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- W2048743965 abstract "Abstract The use of sulphoxides as synergist in the solvent extraction of uranyl ion with β-diketones has been investigated by distribution measurements in the system UO22+/HTTA/S, where S is diphenyl or dibenzyl sulphoxide. Results indicate that the sulphoxides exert only a feeble synergetic action which is several orders of magnitude smaller than that of trioctyl phosphine oxide. Values of the equilibrium constants for the system UO22+/HTTA/S are comparable in magnitude to those of the analogous systems with tributyl phosphate. Solid crystalline complexes of the formula UO2X2S (X = anion of theonoyl trifluoroacetone, acetylacetone or dibenzoyl methane) have been isolated. Infrared and proton nuclear magnetic resonance spectra indicate that both the β-diketone moieties in these systems are bidentate. F19 nuclear magnetic resonance spectra however, does indicate some disymmetry in the molecules, UO2(TTA)2TOPO (TOPO = trioctyl phosphine oxide) and UO2 (TTA)2DBSO (DBSO = dibenzyl sulphoxide). This disymmetry is probably caused by the incorporation of the neutral donor molecule into the complex." @default.
- W2048743965 created "2016-06-24" @default.
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- W2048743965 date "1969-08-01" @default.
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- W2048743965 title "Complexes of uranyl diketones with aromatic sulphoxides" @default.
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- W2048743965 doi "https://doi.org/10.1016/0022-1902(69)80590-7" @default.
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