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- W2048897949 abstract "Abstract An experimental study of 3,3′-bis(azidomethyl) oxetane/3-azidomethyl-3-methyloxetane (BAMO/AMMO) and BAMO/AMMO/TiO 2 was performed to investigate thermal decomposition of the copolymer and the effect of TiO 2 on its decomposition. Experiments were conducted at 0.1 MPa with heat fluxes of 100 and 400 W/cm 2 , delivered by a CO 2 laser. Gaseous samples were extracted by quartz microprobes and analyzed in a triple quadrupole mass spectrometer (TQMS). Gas-phase temperature profiles and surface temperatures were measured using the micro-thermocouple technique to investigate gas-phase reaction zones identified by the species measurement. Species measurements revealed that decomposition products of BAMO/AMMO were quite similar to those reported for BAMO and that the addition of TiO 2 caused no significant changes in mole fractions of the products, except for an increase in NH 3 . Product species were indicative of simultaneous decomposition of the backbone structure and side chains. No evidence of gas-phase reaction was found in gas-phase species or temperature profiles, indicating that the reactions are occurring in the condensed-phase or in a near-surface reaction zone. The regression rate was substantially reduced by the addition of TiO 2 at a heat flux of 400 W/cm 2 . Based upon the species and temperature measurements, it is argued that this reduction is primarily a result of physical, rather than chemical, effects of the TiO 2 ." @default.
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- W2048897949 date "2002-02-01" @default.
- W2048897949 modified "2023-10-01" @default.
- W2048897949 title "Thermal decomposition of BAMO/AMMO with and without TiO2" @default.
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- W2048897949 doi "https://doi.org/10.1016/s0040-6031(01)00785-7" @default.
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